1021019-03-3

  • Product Name:2-bromo-[1,2,4]triazolo[1,5-a]pyridine
  • Molecular Formula:C6H4BrN3
  • Purity:99%
  • Molecular Weight:198.022
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Product Details;

CasNo: 1021019-03-3

Molecular Formula: C6H4BrN3

Factory Sells Best Quality 2-bromo-[1,2,4]triazolo[1,5-a]pyridine 1021019-03-3 with stock

  • Molecular Formula:C6H4BrN3
  • Molecular Weight:198.022
  • PKA:0.47±0.30(Predicted) 
  • PSA:30.19000 
  • Density:1.89±0.1 g/cm3(Predicted) 
  • LogP:1.49180 

1021019-03-3 Relevant articles

ORGANIC COMPOUNDS AND ORGANIC ELECTRO LUMINESCENCE DEVICE COMPRISING THE SAME

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Paragraph 0147; 0158-0162, (2019/08/01)

The present invention relates to a novel...

Triazolopyridine based organic electroluminescent material and organic electroluminescent device

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Paragraph 0064-0065, (2020/01/03)

The invention relates to the technical f...

In order to N - pyridine -2 - (1 H) - [...] for the mother nucleus of the fluorescent molecule and its preparation and use (by machine translation)

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Paragraph 0032; 0034; 0036; 0040, (2018/11/22)

The invention of formula (I) as shown in...

1021019-03-3 Process route

2-amino-s-triazolo-<1,5-a>-pyridne
874-46-4

2-amino-s-triazolo-<1,5-a>-pyridne

2-bromo-[1,2,4]triazolo[1,5-a]pyridine
1021019-03-3

2-bromo-[1,2,4]triazolo[1,5-a]pyridine

Conditions
Conditions Yield
With hydrogen bromide; sodium nitrite; In water; acetonitrile; at 20 ℃; Cooling with ice;
73%
With hydrogen bromide; copper(ll) bromide; sodium nitrite; In tetrahydrofuran; water; at 0 - 20 ℃; for 12h;
60%
With nitrous acid isobutyl ester; copper(ll) bromide; In acetonitrile; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
3.08 g
2-aminopyridine
504-29-0

2-aminopyridine

2-bromo-[1,2,4]triazolo[1,5-a]pyridine
1021019-03-3

2-bromo-[1,2,4]triazolo[1,5-a]pyridine

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: dichloromethane / 4 h / 20 °C
1.2: 20 °C / Reflux
2.1: sodium nitrite; hydrogen bromide / water; acetonitrile / 20 °C / Cooling with ice
With hydrogen bromide; sodium nitrite; In dichloromethane; water; acetonitrile;
Multi-step reaction with 3 steps
1: dichloromethane / 20 h / 0 - 20 °C
2: hydroxylamine hydrochloride; triethylamine / ethanol; methanol / 3 h / Reflux
3: copper(ll) bromide; hydrogen bromide; sodium nitrite / tetrahydrofuran; water / 12 h / 0 - 20 °C
With hydroxylamine hydrochloride; hydrogen bromide; triethylamine; copper(ll) bromide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
Multi-step reaction with 3 steps
1: 20 °C
2: N,N-diethylethylenediamine; hydroxylamine hydrochloride / methanol; ethanol / 2 h / 60 °C
3: copper(ll) bromide; nitrous acid isobutyl ester / acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere
With nitrous acid isobutyl ester; hydroxylamine hydrochloride; N,N-diethylethylenediamine; copper(ll) bromide; In methanol; ethanol; acetonitrile;

1021019-03-3 Upstream products

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