1069-23-4
- Product Name：1,5-Hexadiene-3,4-diol
- Molecular Formula：C6H10O2
- Purity：99%
- Molecular Weight：114.144
Product Details;
CasNo： 1069-23-4
Molecular Formula： C6H10O2
Appearance： Light yellow oily liquid
Offer Chemical Raw Material 1,5-Hexadiene-3,4-diol 1069-23-4 In Stock
- Molecular Formula:C6H10O2
- Molecular Weight:114.144
- Appearance/Colour:Light yellow oily liquid
- Vapor Pressure:0.0737mmHg at 25°C
- Melting Point:14-16 °C(lit.)
- Refractive Index:n20/D 1.479(lit.)
- Boiling Point:201.9 °C at 760 mmHg
- PKA:13.27±0.20(Predicted)
- Flash Point:92.8 °C
- PSA：40.46000
- Density:1.005 g/cm3
- LogP:0.08020
1,5-Hexadiene-3,4-diol(Cas 1069-23-4) Usage
InChI:InChI=1/C6H10O2/c1-3-5(7)6(8)4-2/h3-8H,1-2H2
1069-23-4 Relevant articles
Total synthesis of 1α,25-dihydroxy-2β-(3-hydroxypropoxy)vitamin D3 (ED-71)
Deng, Wutong,Gong, Yimou,Pu, Qingyin,Sun, Jian,Wang, Chao,Zhou, Li
, (2020)
A convergent method for the synthesis of...
Synthesis of the tetracyclic core of exiguaquinol
Schwarzwalder, Gregg M.,Steinhardt, Sarah E.,Pham, Hung V.,Houk,Vanderwal, Christopher D.
, p. 6014 - 6017 (2013)
A Diels-Alder reaction, a desymmetrizing...
ORGANOMETALLIC SYNTHESIS IN AQUEOUS MEDIA. SYNTHESIS OF VINYLALLYLCARBINOLS
Mistryukov, E. A.,Korshevits, I. K.
, p. 2396 - 2397 (1986)
-
Synthesis of highly functional carbamates through ring-opening of cyclic carbonates with unprotected α-amino acids in water
Olsén, Peter,Oschmann, Michael,Johnston, Eric V.,?kermark, Bj?rn
, p. 469 - 475 (2018)
The present work shows that it is possib...
Isocyanate-free route to poly(carbohydrate-urethane) thermosets and 100% bio-based coatings derived from glycerol feedstock
Schmidt, Stanislaus,Ritter, Benjamin S.,Kratzert,Bruchmann, Bernd,Mülhaupt, Rolf
, p. 7268 - 7276 (2016)
Glycerol serves as the exclusive bio fee...
Cyclic allylic carbonates as a renewable platform for protecting chemistry in water
Olsén, Peter,Morvan, Jennifer,Sawadjoon, Supaporn,Shatskiy, Andrey,Johnston, Eric V.,?kermark, Bj?rn
, p. 3186 - 3190 (2018)
The present work explores different cycl...
Large-Scale Synthesis of Eldecalcitol
Moon, Hyung Wook,Lee, Seung Jong,Park, Seong Hu,Jung, Se Gyo,Jung, In A.,Seol, Chang Hun,Kim, Seung Woo,Lee, Seon Mi,Gangganna, Bogonda,Park, Seokhwi,Lee, Kee-Young,Oh, Chang-Young,Song, Juyoung,Jung, Jaehun,Heo, Ji Soo,Lee, Kang Hee,Kim, Hae Sol,Lee, Won Taek,Baek, Areum,Shin, Hyunik
, p. 98 - 107 (2021/01/09)
Industrial-scale synthesis of eldecalcit...
1069-23-4 Process route
-
-
64-19-7,77671-22-8
acetic acid
-
-
107-02-8,25068-14-8
acrolein
-
-
122124-32-7
2-hydroxy-5-vinyltetrahydrofuran
-
-
71-23-8
propan-1-ol
-
-
19700-96-0,19700-97-1,58208-04-1,112571-38-7,144829-86-7,1069-23-4
hexa-1,5-diene-3,4-diol
-
-
107-18-6
allyl alcohol
| Conditions | Yield |
|---|---|
|
|
-
-
107-02-8,25068-14-8
acrolein
-
-
19700-96-0,19700-97-1,58208-04-1,112571-38-7,144829-86-7,1069-23-4
hexa-1,5-diene-3,4-diol
| Conditions | Yield |
|---|---|
|
With
ammonium chloride; zinc;
In
tetrahydrofuran;
|
82% |
|
With
ammonium chloride; zinc;
In
tetrahydrofuran;
|
80% |
|
With
ammonium chloride; zinc;
In
tetrahydrofuran; water;
|
70% |
|
With
ammonium chloride; zinc;
In
tetrahydrofuran; water;
at 20 ℃;
|
70% |
|
With
ammonium chloride; zinc;
In
tetrahydrofuran; water;
for 2h;
|
60% |
|
With
water; acetic acid; zinc;
die filtrierte Loesung wird wiederholt mit Aether ausgeschuettelt;
|
|
|
With
coppered zinc; acetic acid;
Abtrennung aus dem erhaltenen Gemisch mit der meso-Form durch Ueberfuehren in das Bis-phenylurethan, das in Aethanol leichter loeslich ist als das der meso-Form;
|
|
|
With
coppered zinc; acetic acid;
Abtrennung aus dem erhaltenen Gemisch mit der meso-Form durch Anlagerung von Brom und Kochen der entstandenen 1.2.5.6-Tetrabrom-hexandiol-(3.4) vom F:96grad mit Zink und Aethanol;
|
|
|
With
vanadium sulfate; water;
|
|
|
With
copper; zinc;
In
acetic acid;
|
|
|
With
acetic acid; zinc;
|
|
|
With
acetic acid; zinc;
In
ethanol;
|
|
|
With
acetic acid; zinc;
In
tetrahydrofuran;
for 18h;
|
|
|
With
acetic acid; zinc;
In
tetrahydrofuran;
at 20 ℃;
for 18h;
|
1069-23-4 Upstream products
-
107-02-8
acrolein
-
106-95-6
allyl bromide
-
7732-18-5
water
-
64-19-7
acetic acid
1069-23-4 Downstream products
-
4984-85-4
propioin
-
4437-51-8
3,4-hexanedione
-
147-73-9
meso-tartaric acid
-
97-95-0
2-ethyl-1-butanol
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